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Each freeze-thaw cycle creates ice crystals that can physically disrupt peptide structure, and the process concentrates the peptide at the boundary between frozen and unfrozen regions, potentially causing aggregation

ProHealth's cited clinical study (Dosz E et al., Nutraceuticals, 2025) reported a 26.4% improvement in digestive comfort associated with ButyroGen at the ingredient level

This might seem like a small detail, but our team has seen more research compromised by improper storage than almost any other factor

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In those cases, the fix is often part mechanical, part medical, and not just try another pill. This is one reason LL-37 is discussed in stubborn sinus and airway issues, where biofilms can play a part